MS Report from Instrument: LCMS-02 File ..3 2017-05-23 08-40-55\\BIZ2017-523-WYQ11_1.D Tgt Mass (CHM): Injection Date : 23 May 17 2:38 pm +0800 Seq. Line : 76 Sample Name : BIZ2017-523-WYQ11_1 Location : P2-D-05 Acq. Operator : CLJ_701 Inj : 1 Spec. Reported : MS Integration Inj Volume : 3 ul Acq. Method : D:\\chem32\\1\\DATA\\20170523\\20170523 2017-05-23 08-40-55\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\METHODS\\1-POS-3MIN-PROSRSS.M Catalog No : HY-149 Batch#24654 A-RP-186 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C*DAD1 B, Sig=214,4 Ref=off 2.6911.60.7001.5332.165mAU60040020000.5*DAD1 C, Sig=254,4 Ref=off mAU40011.522.52.6913min*1.4461.6662.25000.6372.5622000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701000005000001.522.52.43min*0.511.5 Ion 301.2, MSD1 301.2,Target Mass 300.2 +H Positive, EIC=300.9:301.9 60000400002000000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.522.52.32.6703min22.53min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.70 0.03 4.65 2.66 0.28 ND 1.53 0.04 3.83 1.68 0.23 ND 1.66 0.02 14.43 10.59 0.88 ND 2.17 0.02 3.91 3.40 0.24 ND 2.69 0.03 1605.98 926.25 98.36 301 Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0. 0.02 1.56 0.08 0.15 ND 1.45 0.02 0.51 0.37 0.05 ND 1.67 0.02 1.21 0.88 0.12 ND 2.25 0.02 2.72 0.13 0.27 ND 2.56 0.03 1.37 0.06 0.14 301 2.69 0.03 1008.15 576.37 99.27 301 Integration Results for MSD1 TIC, MS FileLCMS-02 5/23/2017 16:16:25 CLJ_701Page 1 of 3
MS Report from Instrument: LCMS-02|-------|--------|--------------|--------------|--------|------| 2. 0.07 693624.94 131402. 100.00 301 RetTim Width Area Height Area% MS(+)LCMS-02 5/23/2017 16:16:25 CLJ_701Page 2 of 3
MS Report from Instrument: LCMS-02Ret. Time: 2. <<<< POSITIVE SPECTRA >>>> ES-API Positive3500030000250002000015000 299.11000050000200300400500600700800900m/z 301.2LCMS-02 5/23/2017 16:16:25 CLJ_701Page 3 of 3
